Introduction to solid-state NMR of inorganic materials
Graduate School of Technical Sciences at Aarhus University
Objectives of the course:
The course gives a basic introduction to the theory behind solid-state NMR, including anisotropic nuclear spin interactions and multiple-pulse NMR experiments.
Six practical exercises serve as an illustration of the NMR theory. These have their origin in magic-angle spinning, cross-polarization, dipolar recoupling, and multiple-quantum MAS experiments (for quadrupolar nuclei) and illustrate their applications in studies of inorganic materials (e.g., polymers, zeolites/AlPO4’s, and Portland cement-based materials). The exercises are mandatory for all participants and must be concluded by a report. Approval of these reports is a prerequisite for attending the final oral evaluation.
Learning outcomes and competences:
At the end of the course, the student should be able to:
- Describe the basic theory behind solid-state NMR including the most important nuclear spin interactions.
- Describe how solid-state NMR experiments are performed on modern NMR equipment.
- Analyze solid-state NMR spectra by using numerical simulations and determine the nuclear spin interaction parameters describing the structure of a compound.
- Describe the concept of dipolar recoupling and its application to obtain structural information.
- Relate experimental NMR parameters and chemical/atomic structure.
- Discuss which solid-state NMR experiments can be used to shed light on different important structural problems.
Course parameters:
Language: English
Level of course: PhD course
Time of year: Q2 2026
No. of contact hours: 4 – 5 hours per week
Capacity limits: Max 10 participants
Course fee: None
Compulsory program:
The exercises are mandatory for all participants and must be concluded by a report. Approval of these reports is a prerequisite for attending the final oral evaluation. The students may have to give a presentation of a paper or similar during the course.
Course contents:
2 lectures per week,
2 hours of theoretical exercises every second week
3 hours of experimental exercises every second week
Prerequisites:
Bachelor degree in chemistry, physics, or nanoscience or similar.
Type of course/teaching methods:
Lectures, theoretical exercises, laboratory exercises, and student presentations
Literature:
Notes, parts of textbooks, and articles. To be announced at the beginning of the course.
Course homepage:
Will be available at Brightspace
Course assessment:
Approved reports associated with the laboratory exercises. An oral exam (25 min.) based on one of the experimental reports (pass/fail evaluation).
Special comments on this course:
This course will only take place this Fall.
Time: To be decided at the first lecture: Wednesday September 2nd, 14:00 In room 1511-215
Place: Department of Chemistry, Laboratories, 8000 Aarhus C
Course fee:
None.
Registration:
Registration by e-mail to Jørgen Skibsted not later than 7th September 2026.